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论文编号: 122214O120120374
第一作者所在部门: 704组
中文论文题目:
英文论文题目: Hydrothermal synthesis and characterization of NiS flower-like architectures
论文题目英文:
作者: 周海
论文出处:
刊物名称: Particuology
: 2012
: 10
: 6
: 783-788
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摘要: Under the influence of thiocyanate anions (SCN?) and cetyltrimethyl ammonium bromide (CTAB), NiS flower-like architectures were successfully synthesized by a one-step hydrothermal method. The synthesized flower-like architectures, with a multilayered and highly ordered texture, have diameters of several micrometers. X-ray powder diffraction (XRD) shows that the NiS flower-like architectures are rhombohedral crystalline. On the basis of condition-dependent experiments, the diffusion-limited aggregation(DLA) model and cage effect were used to explain the growth process of rhombohedral crystalline NiS flower-like architectures. Magnetic measurements showed that the coercivity (Hc) of the as-obtained NiS flower-like architectures was 102.14 Oe.
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